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Bestimmung von SO2 und H2S mittels Kaliumpermanganat

✍ Scribed by Dr. Erich Boye; Eugen Graner

Publisher
John Wiley and Sons
Year
1948
Tongue
English
Weight
336 KB
Volume
60
Category
Article
ISSN
0044-8249

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Zersetzung von Tetramethylammoniumcyansu
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✍ Andreas Kornath; Oliver Blecher 📂 Article 📅 2002 🏛 John Wiley and Sons 🌐 German ⚖ 405 KB 👁 1 views

Tetramethylammonium cyanosulfite decomposes in SO 2 at Ϫ70 °C to give HCN, [(CH 3 ) 4 N] ϩ HSO 4 Ϫ • SO 2 and [(CH 3 ) 4 N ϩ ] 2 S 2 O 7 2Ϫ • 2 SO 2 . A reaction sequence for the decomposition is discussed. The formed salts are characterized by infrared, Raman spectroscopy, and single crystal X-ray