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Benzo[c]fused isothiazoles. I. synthesis of the angular benzo[c]bisisothiazoles and of the symmetrical benzo[c]trisisothiazole

✍ Scribed by Basil Danylec; Michael Davis

Book ID
112125990
Publisher
Journal of Heterocyclic Chemistry
Year
1980
Tongue
English
Weight
257 KB
Volume
17
Category
Article
ISSN
0022-152X

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## Abstract The synthesis of benzo[a]pyrene‐6‐^13^C is described. Perinaphthane was converted to 6‐benzoyl‐carbonyl‐^13^C‐perinaphthane which was cyclized to 2,3‐dihydrobenzo[a]pyren‐6(1H)‐one‐6‐^13^C. Subsequent reduction of the ketone followed by dehydration and dehydrogenation gave benzo[a]pyren