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Beneficial Effect of TMSCl in the Lewis Acid-Mediated Carboxylation of Aromatic Compounds with Carbon Dioxide.

✍ Scribed by Koji Nemoto; Hiroki Yoshida; Yutaka Suzuki; Naoya Morohashi; Tetsutaro Hattori


Publisher
John Wiley and Sons
Year
2006
Weight
16 KB
Volume
37
Category
Article
ISSN
0931-7597

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COMMUNICATIONS 0.90 -0.80 -0.70 -0.60 -940.8 (3) A' , z = I , p =1.630 gcm-'. p = 2.032 mm-', crystal size 0.20 x 0.20 x 0.40 mm, F(000) = 480.0; 5531 unique reflections and 5468 assumed as observed with 1>2u(l). 268 parameters, R(F,) = 0.0461. R,IF,I\* = 0.1025 and S = 0.966. Crystallographic data