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Beckmann fragmentation reaction of 3-methoxy-17.beta.-hydroxyestra-1,3,5(10)-trien-16-one oxime

✍ Scribed by Miljkovic, Dusan; Petrovic, Julijana

Book ID: 126482863
Publisher: American Chemical Society
Year: 1977
Tongue: English
Weight: 273 KB
Volume: 42
Category: Article
ISSN: 0022-3263
DOI: 10.1021/jo00432a015

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## Abstract The four possible isomers of 16‐hydroxymethyl‐3‐methoxyestra‐1,3,5(10)‐trien‐17‐ol 5a, 6a, 7a, 8a were converted into the corresponding 16‐methyl analogues 4a, 11a, 12a, 13a, which were characterized from their ^1^H‐ and ^13^C‐NMR spectra. The results permit a configurational correlatio