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B(C6F5)3-Catalyzed Silation of Alcohols: A Mild, General Method for Synthesis of Silyl Ethers

✍ Scribed by Blackwell, James M.; Foster, Katherine L.; Beck, Victoria H.; Piers, Warren E.

Book ID: 115494701
Publisher: American Chemical Society
Year: 1999
Tongue: English
Weight: 76 KB
Volume: 64
Category: Article
ISSN: 0022-3263
DOI: 10.1021/jo9903003

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The primary alcohols lad and ethers 4a-b were effectively reduced into the corresponding hydrocarbons 2 by HSiEt3 in the presence of catalytic amounts of B(C6F5)3. The secondary alkyl ethers 4g,h underwent cleavage and/or reduction under similar reaction conditions to produce either the silyl ether