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A Novel B(C 6 F 5 ) 3 -Catalyzed Reduction of Alcohols and Cleavage of Aryl and Alkyl Ethers with Hydrosilanes †

✍ Scribed by Gevorgyan, Vladimir; Rubin, Michael; Benson, Sharonda; Liu, Jian-Xiu; Yamamoto, Yoshinori

Book ID
120159908
Publisher
American Chemical Society
Year
2000
Tongue
English
Weight
271 KB
Volume
65
Category
Article
ISSN
0022-3263

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The primary alcohols lad and ethers 4a-b were effectively reduced into the corresponding hydrocarbons 2 by HSiEt3 in the presence of catalytic amounts of B(C6F5)3. The secondary alkyl ethers 4g,h underwent cleavage and/or reduction under similar reaction conditions to produce either the silyl ether

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HSiR 3 /cat-B(C 6 F) 3 induced dealkylation or reduction of esters of phosphorus at 20°C. A specific conversion to P-silylesters occurred by reaction with tertiary silanes. In contrast, free phosphines were observed in the reaction with mono-or disubstituted silanes. A mechanism was proposed to rati

ChemInform Abstract: A Novel Reduction o
ChemInform Abstract: A Novel Reduction of Alcohols and Ethers with a HSiEt3/Catalytic B(C6F5)3 System.
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