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Azonia-azulene salts. Part 5. Synthesis of 5H-pyrrolo[1,2-a]azepine and of 7H-pyrrolo[1,2-a]azepin-7-one

✍ Scribed by Jones, Gurnos; Radley, Peter M.

Book ID
121298731
Publisher
Royal Society of Chemistry
Year
1982
Weight
998 KB
Category
Article
ISSN
1472-7781

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## Abstract Fused tricyclic 7‐phenyl‐5__H__‐thizolo[5,4‐__e__]pyrrolo[1,2‐__a__][1,4]diazepin‐10(9__H__)one (**10**) was prepared by thermolysis of 2‐phenyl‐4‐(1‐pyrrolylmethyl)thiazole‐5‐carbonyl azide (**9**) in acetic acid. In addition, starting from **10**, 7‐phenyl‐5__H__‐thiazolo [5,4‐__e__][

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The title compound, C~18~H~17~NO~2~, synthesized from enantiomerically pure L-proline, methyl chloroformate and a Grignard reagent, crystallizes with two molecules in the asymmetric unit. A chair conformation is adopted by the two fused five-membered rings.