Three new monomeric complexes of palladium(II) azide with 2-chloropyridine (1), 3-chloropyridine (2), and quinoline (3), have been synthesized by reaction of palladium nitrate and the respective Lewis-base with sodium azide in a water/acetone mixture. All three compounds were characterized by IR, Ra
Azido Complexes of Manganese(II) and palladium(II)
β Scribed by Priv.-Doz. Dr. W. Beck; Dipl.-Chem. K. Feldl; Dr. E. Schuierer
- Publisher
- John Wiley and Sons
- Year
- 1965
- Tongue
- English
- Weight
- 242 KB
- Volume
- 4
- Category
- Article
- ISSN
- 0044-8249
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Palladium(II) azide (1) was synthesized by reaction of palladate(II) (3) were synthesized by a high-yield reaction. Both were characterized by X-ray structural analysis, IR, palladium nitrate and sodium azide. 1 was characterized by AAS, IR, and 14 N-NMR spectroscopy. Bis(azido)bis(pyridine)-Raman,