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Autoxidation of hydrazine with manganese(III)-hematoporphyrin

✍ Scribed by Ichiro Okura; Nguyen Kim Thuan; Tominaga Keii

Publisher
Elsevier Science
Year
1979
Weight
307 KB
Volume
5
Category
Article
ISSN
0304-5102

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Synthesis of 4,4-bis(2-hydroperoxyalkyl)pyrazolidine-3,5-diones using manganese(III)-catalyzed autoxidation
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The autoxidation of a mixture of 1,2-disubstituted pyrazolidine-3,5-diones 1 and alkenes 2 in the presence of a catalytic amount of manganese(III) acetate dihydrate in air gave 4,4-bis(2-hydroperoxyalkyl)pyrazolidine-3,5-diones 3 in 75-96% yields. The structure of the bis(2-hydroperoxyethyl)pyrazoli