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Attogram-level detection and relative sensitivity of strong electrophores by gas chromatography with electron capture detection

✍ Scribed by Corkill, Jeffrey A.; Joppich, Markus.; Kuttab, Simon H.; Giese, Roger W.


Book ID
127085888
Publisher
American Chemical Society
Year
1982
Tongue
English
Weight
718 KB
Volume
54
Category
Article
ISSN
0003-2700

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Electrophore-labeling and alkylation of
✍ Albert Nazareth; Markus Joppich; Samy Abdel-Baky; Kathleen O'Connell; Abdellah S πŸ“‚ Article πŸ“… 1984 πŸ› Elsevier Science 🌐 English βš– 704 KB

The pyrimidine bases cytosine, uracil and thymine, along with some analogues, are electrophore-labeled either with pentafluorobenzoyl chloride (PFBC), pentafluorophenylsulfonyl chloride (PPSC), or heptafluorobutyric anhydride. Subsequent alkylation is most successful for PFB-cytosine, PPS-uracil, an