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Asymmetric Vinylogous Diels-Alder Reactions Catalyzed by a Chiral Phosphoric Acid

✍ Scribed by Tian, Xu; Hofmann, Nora; Melchiorre, Paolo

Book ID: 121650594
Publisher: John Wiley and Sons
Year: 2014
Tongue: English
Weight: 499 KB
Volume: 53
Category: Article
ISSN: 0044-8249
DOI: 10.1002/anie.201310487

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Reaction of Cis Hydroxy Epoxide 63 with Dimsylpotassium. Preparat ion of ( 1 S *, 1 'S * ,3'R * ,8'S *) -1 -(2',7'-Dioxabic y clo[ 4.4.01decan-3'yl)-2-propanol (65) and Its Acetate ( ). The bicyclic compound 65 was prepared from compound 63 (19.8 mg, 0.1 mmol) by the same procedure used to convert 6