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Asymmetric Synthesis of 2-Amino-1,3-diols and D-erythro-Sphinganine.

✍ Scribed by Dieter Enders; Anke Mueller-Huewen

Publisher
John Wiley and Sons
Year
2004
Weight
193 KB
Volume
35
Category
Article
ISSN
0931-7597

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✦ Synopsis

Abstract

For Abstract see ChemInform Abstract in Full Text.

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## Abstract A five‐step synthesis of DL‐erythro‐2‐acetamino‐octadecan‐1,3‐diol (IXb) from palmitoic acid was realised. Palmitoic acid was converted into 2‐bromo‐palmitoylbrornide (11), this, in turn, condensed with ethyl diazoacetate into ethyl 2‐diazo‐3‐oxo‐4‐bromostearate (IV), which furnished on