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Asymmetric hydrogenation of oxime of diethyl ester ofα- ketoglutaric acid

✍ Scribed by T. R. Popova; S. L. Davydova; N. A. Platé

Book ID
112421288
Publisher
Springer
Year
1972
Tongue
English
Weight
52 KB
Volume
21
Category
Article
ISSN
1573-9171

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Asymmetric catalytic hydrogenation of methyl phenylglyoxylate with diamine-chelated metal was studied. Enantiomeric excesses of up to 50% were obtained using a rhodium complex prepared in situ by mixing bis(l,5-cyclooctadiene)dirhodium(I) dichloride with two equivalents of (N,N')dimethyl (1 R,2R)di