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Asymmetric Formal Synthesis of (+)-Lactacystin

โœ Scribed by Sridhar, Chirumarry; Vijaykumar, Bodduri V. D.; Radhika, Laghuvarapu; Shin, Dong-Soo; Chandrasekhar, Srivari

Book ID
127317393
Publisher
John Wiley and Sons
Year
2014
Tongue
English
Weight
293 KB
Volume
2014
Category
Article
ISSN
1434-193X

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Catalytic Asymmetric Total Synthesis of
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Catalytic Asymmetric Total Synthesis of (+)-Lactacystin (I).
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An enantioselective formal synthesis of
An enantioselective formal synthesis of the proteasome inhibitor (+)-lactacystin
โœ Martin P. Green; Jeremy C. Prodger; Christopher J. Hayes ๐Ÿ“‚ Article ๐Ÿ“… 2002 ๐Ÿ› Elsevier Science ๐ŸŒ French โš– 64 KB

An enantioselective formal synthesis of the proteasome inhibitor (+)-lactacystin has been achieved using an alkylidene carbene 1,5-CH insertion reaction as a key step. The key cyclisation precursor was synthesised in high diastereomeric excess using a combination of known procedures, with the two ke