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Asymmetric Aldol Reaction of Enol Trichloroacetate Catalyzed by Tin Methoxide and BINAP×Silver(I) Complex.

✍ Scribed by Akira Yanagisawa; Yukari Matsumoto; Kenichi Asakawa; Hisashi Yamamoto

Publisher
John Wiley and Sons
Year
2003
Weight
227 KB
Volume
34
Category
Article
ISSN
0931-7597

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(S,S)-Ethylenebis(tetrahydroindenyl)titanium chloride methoxide, (S, S)-(EBTHI)TiCl(OMe) (3) was synthesized from the corresponding titanium dichloride. The asymmetric aldol reaction of enol trichloroacetate of cyclohexanone 1 with aromatic aldehydes was studied in the presence of a catalytic amount