𝔖 Bobbio Scriptorium
✦   LIBER   ✦

Applications of INEPT experiments for 119Sn NMR spectroscopy

✍ Scribed by Véronique Gouron; Bernard Jousseaume; Max Ratier; Jean-Claude Lartigue; Michel Petraud

Publisher
John Wiley and Sons
Year
1990
Tongue
English
Weight
324 KB
Volume
28
Category
Article
ISSN
0749-1581

No coin nor oath required. For personal study only.

✦ Synopsis

Abstract

The application of a non‐refocusing INEPT pulse sequence in ^119^Sn NMR spectroscopy allows the determination of ^n^J(^119^Sn, ^1^H) values by comparison of the observed patterns with calculated spectra. It gives an easy access to ^n^J(^119^Sn, ^1^H) values in butyltin derivatives.

📜 SIMILAR VOLUMES

119/117/115Sn low-abundance single-trans
119/117/115Sn low-abundance single-transition correlation spectroscopy (LASSY): sensitivity-enhanced homonuclear correlation experiments for Sn NMR
✍ Christy George; Narayanan Chandrakumar 📂 Article 📅 2010 🏛 John Wiley and Sons 🌐 English ⚖ 275 KB

## Abstract We report the implementation of our novel rare‐spin homonuclear correlation experiment, namely, Low‐Abundance Single‐transition correlation SpectroscopY (LASSY), for ^119/117/115^Sn NMR at natural abundance. Our pulse sequence results in diagonal suppressed COSY‐style display and outper

Combined DEPT 1D and INEPT DQF COSY 2D E
Combined DEPT 1D and INEPT DQF COSY 2D Experiments in 29Si NMR Spectroscopy of Alkoxysilane Polymers. 2—Applications of 29Si NMR to Polymerisation Reactions in Dimethyldiethoxysilane.
✍ P. Lux; F. Brunet; J. Virlet; B. Cabane 📂 Article 📅 1996 🏛 John Wiley and Sons 🌐 English ⚖ 545 KB

Polymerization reactions in dimethyldiethoxylsilane were studied using a new high-resolution 29Si NMR method. This method is a combination of two polarization transfer experiments (DEPT) with a 29Si-29Si two-dimensional INEPT DQF COSY NMR experiment. The structures of oligomers were identified, incl