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Application of two-dimensional correlated NMR techniques to the structure elucidation of 1-methoxy-endo-tetracyclo[6.3.0.02,11.03,7]- undec-9-ene

✍ Scribed by C. Kruk; A. W. H. Jans; J. Cornelisse; J. Lugtenburg

Publisher: John Wiley and Sons
Year: 1985
Tongue: English
Weight: 297 KB
Volume: 23
Category: Article
ISSN: 0749-1581
DOI: 10.1002/mrc.1260230906

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✦ Synopsis

By meam of 5OOMHz 'H two-dimensional correlated NMR spectroscopy and the 62.89--C two-dimemional hadequate technique, all proton and carbon cbemid shifts of 1-methoxy-endetetracy-cl0[6.3.0.@''.@~]undec-9-ene can be assigned m an unambiguous way.

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✍ A. W. H. Jans; J. Lugtenburg; J. Cornelisse; C. Kruk 📂 Article 📅 1982 🏛 John Wiley and Sons 🌐 English ⚖ 270 KB 👁 1 views

## Abstract High field NMR spectroscopy, including nuclear Overhauser effect experiments and homonuclear decoupling techniques, provide conclusive evidence for the structure of 1‐methoxy‐__endo__‐tetracyclo[6.3.0.0^2,11^.0^3,7^]undec‐9‐enundec‐9‐ene. The ^13^C NMR spectrum has been recorded and the