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Application of matrix solid phase dispersion for the determination of clenbuterol in liver samples

✍ Scribed by D. Boyd; P. Shearan; J.P. Hopkins; M. O'Keeffe; M.R. Smyth

Publisher
Elsevier Science
Year
1993
Tongue
English
Weight
483 KB
Volume
275
Category
Article
ISSN
0003-2670

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✦ Synopsis

A rapId method for determmation of clenbuterol m hver samples has been developed It mvolves combmmg matnx sohd phase dlsperslon with radlommmnoassay as an efficxent techmque for residue determmatlon at the sub ng g-' level The techmque was optmnsed for extract clean-up and recovery of residue usmg radiolabelled [3H&c1enbuterol Inter-and mtra-assay vahdation, camed out on fortified bver samples, showed high recovenes over the range l-5 ng clenbuterol g-' The determmatlon of mcurred residues m hver samples has been mvestlgated Tbe developed procedure allows for determmatlon of residues of clenbuterol m &sues at levels of less than 0 5 ng g-'

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