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Application of Hemithio Ketene Acetals to the Synthesis of Spirocyclic Orthoesters.

✍ Scribed by Thomas E. La Cruz; Scott D. Rychnovsky

Book ID
101961906
Publisher
John Wiley and Sons
Year
2005
Weight
18 KB
Volume
36
Category
Article
ISSN
0931-7597

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A new method for the synthesis of mixed
A new method for the synthesis of mixed orthoesters from O-allyl acetals
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Two new methods for the synthesis of orthoesters and compounds containing an orthoester moiety (dihydroisoxazoles) are presented. Mixed orthoesters of general formulas RC(OR 1 )(OR 2 ) 2 and RC(OR 1 )-(OR 2 )(OR 3 ) were prepared via addition of ROH (R = Bu or m-methylphenyl) to O-allyl acetals (acr