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Application of cyclic sulfates in the synthesis of 6-deoxy-d-manno-heptopyranose derivatives

✍ Scribed by Pieter A.M. van der Klein; Jacques H. van Boom

Book ID: 102999450
Publisher: Elsevier Science
Year: 1992
Tongue: English
Weight: 631 KB
Volume: 224
Category: Article
ISSN: 0008-6215
DOI: 10.1016/0008-6215(92)84105-2

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✦ Synopsis

6-Deoxy-D-manno-heptopyranose was prepared in five steps starting from methyl 2,3-O-isopropylidene-alpha-D-mannopyranoside 4,6-sulfate or methyl 2,3-O-isopropylidene-alpha-D-mannofuranoside 5,6-sulfate. The glycosyl donor ethyl 2,3,4,7-tetra-O-benzoyl-6-deoxy-1-thio-alpha,beta-D-manno- heptopyranoside was used to synthesize methyl 4-O-(6-deoxy-alpha-D-manno-heptopyranosyl)-beta-D-galactopyranoside.

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