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Anodic Cyclization Reactions: The Total Synthesis of Alliacol A

✍ Scribed by Mihelcic, John; Moeller, Kevin D.

Book ID: 120820357
Publisher: American Chemical Society
Year: 2003
Tongue: English
Weight: 56 KB
Volume: 125
Category: Article
ISSN: 0002-7863
DOI: 10.1021/ja029064v

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## Abstract For Abstract see ChemInform Abstract in Full Text.

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A synthesis of (À)-crobarbatic acid is reported along with the first use of a vinyl-substituted ketene dithioacetal as a coupling partner for an anodic cyclization reaction. The use of the vinyl-substituted ketene dithioacetal enables the construction of a cyclic product having a tetrasubstituted ca

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The anodic coupling of an enol ether to an oxygen nucleophile has been used as a key step in the total synthesis of (+)-nemorensic acid. The anodic cyclization reaction allows for a reversal in the way the tetrahydrofuran ring of the natural product is normally assembled and thus enables constructio