Annealing and characterisation of TlBr crystals for detector applications
✍ Scribed by V. Kozlov; M. Leskelä; H. Sipilä
- Book ID
- 108219189
- Publisher
- Elsevier Science
- Year
- 2005
- Tongue
- English
- Weight
- 199 KB
- Volume
- 546
- Category
- Article
- ISSN
- 0168-9002
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The combination of distillation, Bridgman-Stockbarger, hydrothermal recrystallisation and travelling molten zone (TMZ) methods were used for TlBr purification. Grown crystals were characterised by XRD rocking curve and FTIR spectroscopy methods, and by electrical measurements made from 200 to 300 K.
The results of the development of the TlBr crystals growth technology are presented. For the purification of the TlBr salts, the combination of the vacuum distillation (VD) methods and directed crystallization (DC) was applied. The processes of the vacuum distillation were made in the vertical one-