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Anilinium 3-methyl-1,2-buta­dienyl-1,1-di­phos­phonate(1–)

✍ Scribed by Angelov, Christo M. ;Heever, Johan P. van den ;McDonald, Robert ;McEwan, Alexander J. B. ;Mercer, John R.


Publisher
International Union of Crystallography
Year
2002
Tongue
English
Weight
266 KB
Volume
58
Category
Article
ISSN
1600-5368

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2-{4-[4-(Di­methyl­amino)­phenyl]-1,3-bu
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2-(3-Methyl-1,2-buta­dienyl)-2-oxo-1,3,2
✍ Angelov, Christo M. ;Mazzuca, Dean A. ;Heever, Johan P. van den ;McDonald, Rober 📂 Article 📅 2002 🏛 International Union of Crystallography 🌐 English ⚖ 252 KB

The structure of the title compound, C 8 H 14 NO 2 P, the ®rst of a compound containing a 1,2-butadienyl group bound to the phosphorus of a 1,3,2-oxazaphosphorinane ring, is reported. ## Experimental Compound (2) was recrystallized from THF to give light-yellow crystals, with m.p. 383 K; 31 P NMR