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Analysis of Oligosaccharide Conformation by NMR Spectroscopy Utilizing 1 H, 1 H and 1 H, 13 C Residual Dipolar Couplings in a Dilute Liquid Crystalline Phase

✍ Scribed by Lycknert, Kristina; Maliniak, Arnold; Widmalm, Göran


Book ID
127185277
Publisher
American Chemical Society
Year
2001
Tongue
English
Weight
54 KB
Volume
105
Category
Article
ISSN
1089-5639

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## Abstract A high‐resolution, phase‐sensitive, natural abundance __F__~2~‐coupled ^1^H–^13^C HSQC (F2HSQC) NMR experiment was developed to measure simultaneously both ^__n__^__D__~HH~ and ^1^__D__~CH~ residual dipolar couplings (RDCs) of small molecules present in a chiral polypeptide liquid cryst