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Analysis of acidic pesticides using in situ derivatization with alkylchloroformate and solid-phase microextraction (SPME) for GC–MS

✍ Scribed by Trine Henriksen; Bo Svensmark; Bo Lindhardt; René K Juhler

Book ID: 117248600
Publisher: Elsevier Science
Year: 2001
Tongue: English
Weight: 175 KB
Volume: 44
Category: Article
ISSN: 0045-6535
DOI: 10.1016/s0045-6535(00)00532-4

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## Abstract This paper described a novel approach for the determination of bisphenol A by dispersive liquid‐phase microextraction with __in situ__ acetylation prior to GC‐MS. In this derivatization/extraction method, 500 μL acetone (disperser solvent) containing 30.0 μL chlorobenzene (extraction so