An Unusual AnionβΟ Interaction in an ;ri
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Jamal Moussa; Vincent Gandon; Marie Noelle Rager; Max Malacria; Lise-Marie Chamo
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Article
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2009
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John Wiley and Sons
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English
β 360 KB
## Abstract The organometallic assembly [Cp\*Ir(Ξ·^6^βC~6~H~2~O~4~)(BF~2~)~2~(CF~3~SO~3~)][Cp\*Ir(ΞΌβCl)~3~IrCp\*] (3) was prepared from [Cp\*Ir(solvent)~3~][OTf]~2~ (2) and 1,2,4,5 tetrahydroxybenzene (THB, 1) in acetone, in the presence of an excess amount of BF~3~Β·2H~2~O. Assembly 3 was fully char