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Synthesis and crystal structure of an unusual mixed crystal containing an oxorhenium(V) and imidorhenium(V) complex

✍ Scribed by P. Mayer; E. Hosten; T. I. A. Gerber; I. Booysen

Book ID
113009477
Publisher
Iranian Chemical Society
Year
2010
Tongue
English
Weight
189 KB
Volume
7
Category
Article
ISSN
1735-207X

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Synthesis and Structural Characterizatio
Synthesis and Structural Characterization of Mixed-Ligand Oxorhenium(V) Complexes Containing Bidentate Dithioethers and Monothiolato Ligands
✍ Reisgys, Martina ;Spies, Hartmut ;Johannesn, Bernd ;Pietzsch, Hans-Jergen ;Leibn πŸ“‚ Article πŸ“… 1997 πŸ› Wiley (John Wiley & Sons) 🌐 English βš– 493 KB πŸ‘ 1 views

Neutral oxorhenium(V) complexes with dithioether ligands of the general formula [ReOX3(RS[CHz]2SR)], X = C1, Br, R = nBu, Et, Bzl were synthesized. Ammonium perrhenate reacts in concentrated hydrochloric acid with dithiaalkanes (RS[CH2I2SR, R = nBu, Et, Bzl) dissolved in glacial acetic acid to give