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An unusual reaction of azide with nitroolefins

✍ Scribed by Shmaryahu Hoz; Dov Speizman

Book ID
104238066
Publisher
Elsevier Science
Year
1979
Tongue
French
Weight
128 KB
Volume
20
Category
Article
ISSN
0040-4039

No coin nor oath required. For personal study only.

✦ Synopsis

The reaction of sodium azide in DMSO with 9-dinitromethylenefluorene (DNF) and 9-bromonitromethylenefluorene (BNF) results in the formation of N-cyano-9-iminofluorene (2). The overall reaction time is two minutes at room temperature.

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