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An oxidation-adsorption method for the analysis of methyl ester fractions

✍ Scribed by H. A. Schuette; Stephen Dal Nogare


Book ID
112824446
Publisher
Springer-Verlag
Year
1951
Tongue
English
Weight
585 KB
Volume
28
Category
Article
ISSN
0003-021X

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An improved on-line synthesis of the powerful methylation reagent, ["CH,]methyl triflate, 1, is described. ## By means of a simple and cheap column technique this reagent is synthesized in an overall reaction time of 12 min in reproducible radiochemical yields of 90% (based on "CO,), a radiochemi