๐”– Bobbio Scriptorium
โœฆ   LIBER   โœฆ

An Odorless, One-Pot Synthesis of Thioesters from Organic Halides, Thiourea and Benzoyl Chlorides in Water

โœ Scribed by Lu, Guo-ping; Cai, Chun

Book ID
120275538
Publisher
John Wiley and Sons
Year
2013
Tongue
English
Weight
370 KB
Volume
355
Category
Article
ISSN
1615-4150

No coin nor oath required. For personal study only.

๐Ÿ“œ SIMILAR VOLUMES

A one-pot, efficient, and odorless synth
A one-pot, efficient, and odorless synthesis of symmetrical disulfides using organic halides and thiourea in the presence of manganese dioxide and wet polyethylene glycol (PEG-200)
โœ Habib Firouzabadi; Nasser Iranpoor; Mohammad Abbasi ๐Ÿ“‚ Article ๐Ÿ“… 2010 ๐Ÿ› Elsevier Science ๐ŸŒ French โš– 158 KB

Primary, secondary, tertiary, allylic, and benzylic halides are converted efficiently into symmetric disulfides in high yields using thiourea as the sulfur atom source. The reactions are odorless and are performed at 30-35 ยฐC in wet PEG-200 using MnO 2 as an oxidant.