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An improved N2O-method for measuring Cu-dispersion

โœ Scribed by J.R Jensen; T Johannessen; H Livbjerg


Book ID
103811647
Publisher
Elsevier Science
Year
2004
Tongue
English
Weight
170 KB
Volume
266
Category
Article
ISSN
0926-860X

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3'-0Acetylthymidine (I) was converted to the 0-acetoxy aldehyde (3) using a modified Swern oxidation procedure. The crude product was reduced with sodium borodeuteride to give, after chromatography, [5'-2H]-3'-CL-acety1thymidine (4) in 68% overall yield from -1. The extent of deuterium incorporation