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An Efficient Procedure for Tri(2-Methoxyphenyl)Phosphine

โœ Scribed by Brandsma, L.; Verkruijsse, H. D.


Book ID
121316209
Publisher
Taylor and Francis Group
Year
1990
Tongue
English
Weight
108 KB
Volume
20
Category
Article
ISSN
0039-7911

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A Procedure for Quantitative Determinati
โœ J.C. Han; G.Y. Han ๐Ÿ“‚ Article ๐Ÿ“… 1994 ๐Ÿ› Elsevier Science ๐ŸŒ English โš– 474 KB

The concentration of tris(2-carboxyethyl)phosphine (TCEP) can be conveniently determined by measuring the amount of 2-nitro-5-thiobenzoate (NTB) formed after reaction with \(5,5^{\prime}\)-dithiobis(2-nitrobenzoic acid) (DTNB). This method utilizes the fact that TCEP reduces DTNB rapidly and stoichi