An efficient one-pot synthesis of substituted 2-arylbenzo[b]thiophene derivatives
β Scribed by Meena V Patel; Jeffrey J Rohde; Vijaya Gracias; Teodozyj Kolasa
- Publisher
- Elsevier Science
- Year
- 2003
- Tongue
- French
- Weight
- 142 KB
- Volume
- 44
- Category
- Article
- ISSN
- 0040-4039
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β¦ Synopsis
This communication describes an efficient one-pot procedure for the synthesis of 2-arylbenzo[b]thiophene derivatives via reaction of o-halo or nitro aryl carbonyl compounds with benzyl mercaptans in the presence of an excess of anhydrous K 2 CO 3 at elevated temperature.
π SIMILAR VOLUMES
## Abstract An efficient one pot access to variously substituted thieno[2,3β__b__]thiophene is described. The title compounds were obtained from 1,3βdicarbonyl or equivalent compounds, carbon disulfide and halomethyl derivatives in good to high yields and fully characterized.