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An Efficient One-Pot Synthesis of N-Methoxy-N-methylamides from Carboxylic Acids.

✍ Scribed by Misoo Kim; Hagyoung Lee; Ki-Jong Han; Kwang-Yol Kay

Publisher
John Wiley and Sons
Year
2004
Weight
82 KB
Volume
35
Category
Article
ISSN
0931-7597

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Mono-N-ethylated h-amino acid esters are obtained in high yields using reductive amination procedures. Formation of imine is achieved by excess of acetaldehyde, followed by removal of acetaldehyde and reduction by NaBH(OAc) 3 . The elaborated one-pot synthesis allows for the efficient synthesis of s