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An approach to pseudomonic acids from acetylenic precursors: synthesis of 2-(hydroxymethyl)-3-butyn-1-ol

✍ Scribed by Bates, Hans Aaron; Farina, James; Tong, Michael

Book ID: 120284304
Publisher: American Chemical Society
Year: 1986
Tongue: English
Weight: 775 KB
Volume: 51
Category: Article
ISSN: 0022-3263
DOI: 10.1021/jo00364a003

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In Scheme 4 on page 3278, structures 5a and 5b are incorrectly given. The correct scheme is printed below. Scheme 4. (a) Pd/C, H 2 , MeOH; (b) pyridineϪSO 3 , DMSO, Et 3 N, CH 2 Cl 2 ; (c) 9, tBuOK, THF, Ϫ78°C; (d) PtO 2 , H 2 , EtOH; (e) Na/NH 3 , EtOH, Ϫ78°C to room temp.; (f) 10% Pd/C, H 2 , 1 