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An antitumor agent, 2-(3,3-dimethyl-1-triazeno)phenyl-1-carboxamide

✍ Scribed by Edwards, S. L. ;Chapuis, G. ;Templeton, D. H. ;Zalkin, A.


Book ID
114523888
Publisher
International Union of Crystallography
Year
1977
Weight
266 KB
Volume
33
Category
Article
ISSN
0567-7408

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Reaction of dimethylamine 14C with a four-fold molar excess of 5-diazoimidazole-4-carboxamide in methanol followed by column chromatography of the product on basic a1 umina afforded 5-3,3-dimethyl-4C-l-triazeno)imi datole-4-carboxamide in 70-75% yield and greater than 99.9% radiochemical purity. The