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An Alternative Synthesis of the Antineoplastic Nucleoside 4‘-ThioFAC and Its Application to the Synthesis of 4‘-ThioFAG and 4‘-Thiocytarazid

✍ Scribed by Yoshimura, Yuichi; Endo, Mikari; Miura, Shinji; Sakata, Shinji

Book ID
126465193
Publisher
American Chemical Society
Year
1999
Tongue
English
Weight
123 KB
Volume
64
Category
Article
ISSN
0022-3263

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An improved preparation of 4-ethynylpyri
An improved preparation of 4-ethynylpyridine and its application to the synthesis of linear bipyridyl ligands
✍ Neil R. Champness; Andrei N. Khlobystov; Alexander G. Majuga; Martin Schröder; N 📂 Article 📅 1999 🏛 Elsevier Science 🌐 French ⚖ 212 KB

A convenient synthesis of 4-ethynylpyridine, 5, starting from 4-vinylpyridine has been developed. Compound 5 reacts readily with pyridyl-and aryl-iodides to give the linear bidentate ligands 7, 9, and 11 in excellent yields.