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Aminomethylation of Organic Halides Promoted by Zinc in Protic Medium.

✍ Scribed by Idalia H. S. Estevam; Margarete F. da Silva; Lothar W. Bieber

Book ID
101983186
Publisher
John Wiley and Sons
Year
2006
Weight
21 KB
Volume
37
Category
Article
ISSN
0931-7597

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Barbier-type organometallic reactions of nitrobenzene with organic halides in protic solvents produce directly N,N-dialkylanilines. With allyl bromide, best yields are obtained using zinc in an aqueous monobasic sodium phosphate solution in the presence of cuprous iodide or tin in methanol. The latt