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Amine-Catalyzed Direct Aldol Reactions of Hydroxy- and Dihydroxyacetone: Biomimetic Synthesis of Carbohydrates

✍ Scribed by Popik, Oskar; Pasternak-Suder, Monika; Leśniak, Katarzyna; Jawiczuk, Magdalena; Górecki, Marcin; Frelek, Jadwiga; Mlynarski, Jacek

Book ID
121854694
Publisher
American Chemical Society
Year
2014
Tongue
English
Weight
706 KB
Volume
79
Category
Article
ISSN
0022-3263

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Synthesis and stereoselective aldol reaction of dihydroxyacetone derivatives
✍ Kwan Soo Kim; Sung Don Hong 📂 Article 📅 2000 🏛 Elsevier Science 🌐 French ⚖ 155 KB

Ecient synthetic methods for 1,3-di-O-benzyldihydroxyacetone (3) and 1,3-O-cyclohexylidenedihydroxyacetone (8) were developed. TiCl 4 -mediated aldol reaction of the silyl enol ether of 3 with aldehydes gave syn aldol products while the reaction of the silyl enol ether of 8 with aldehydes aorded ant