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Aluminacyclopentanes in the Synthesis of Ethyl 1-Hydroxycyclopentanecarboxylates.

✍ Scribed by U. M. Dzhemilev; A. G. Ibragimov; L. O. Khafizova; R. R. Gilyazev; A. L. Makhamatkhanova

Publisher
John Wiley and Sons
Year
2007
Weight
22 KB
Volume
38
Category
Article
ISSN
0931-7597

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## Abstract A scheme is developed for synthesizing ^14^C labelled α‐acetates of secondary α‐hydroxylated nitrosamines. In this manner ^14^C‐methyl (1‐acetoxy)ethyl nitrosamine and 1‐^14^C‐ethyl (1‐acetoxy)ethyl nitrosamine are synthesized in 16.3 and 33.3% yield, radiochemically pure.