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Alternative Synthesis of 2-Hydroxy-3,5,5-trimethylcyclopent-2-en-1-one

✍ Scribed by Christian Chapuis; Christine Saint-Léger

Publisher: John Wiley and Sons
Year: 2010
Tongue: German
Weight: 168 KB
Volume: 93
Category: Article
ISSN: 0018-019X
DOI: 10.1002/hlca.200900231

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✦ Synopsis

14.9 (q).

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## Abstract The title cyclohexenone **1d** undergoes photodimerization selectively at the exocyclic CC bond to give a 1 : 1 mixture of 1,2‐dialkynyl‐1,2‐dimethylcyclobutanes **6** and **7**. On irradiation in the presence of 2,3‐dimethylbuta‐1,3‐diene, **1d** affords bicyclo[8.4.0]tetradeca‐1,2,3,