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Alternative Synthesis of 2-Hydroxy-3,5,5-trimethylcyclopent-2-en-1-one

✍ Scribed by Christian Chapuis; Christine Saint-Léger


Publisher
John Wiley and Sons
Year
2010
Tongue
German
Weight
168 KB
Volume
93
Category
Article
ISSN
0018-019X

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✦ Synopsis


14.9 (q).


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Photocycloaddition Reactions of 5,5-Dime
✍ Inga Inhülsen; Jürgen Kopf; Paul Margaretha 📂 Article 📅 2008 🏛 John Wiley and Sons 🌐 German ⚖ 197 KB

## Abstract The title cyclohexenone **1d** undergoes photodimerization selectively at the exocyclic CC bond to give a 1 : 1 mixture of 1,2‐dialkynyl‐1,2‐dimethylcyclobutanes **6** and **7**. On irradiation in the presence of 2,3‐dimethylbuta‐1,3‐diene, **1d** affords bicyclo[8.4.0]tetradeca‐1,2,3,