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Alternative method for gas chromatography-mass spectrometry analysis of short-chain fatty acids in faecal samples

✍ Scribed by Rocio García-Villalba; Juan A. Giménez-Bastida; Maria T. García-Conesa; Francisco A. Tomás-Barberán; Juan Carlos Espín; Mar Larrosa

Book ID
118763401
Publisher
John Wiley and Sons
Year
2012
Tongue
English
Weight
601 KB
Volume
35
Category
Article
ISSN
1615-9306

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Isotope dilution gas chromatographic mass spectrometric assays were developed for the concentration of shortchain fatty acids and of lactate in plasma. The assays involve spiking the samples with 'Hand/or "C-labeled internal standards and direct derivatization with 2,4difluoroaniline, using 1,3-dicy