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Alkyne Complexes of Rhenium in Intermediate Oxidation States; Synthesis and Molecular Structure of a Rhenium(V)-Allenylidene Complex

✍ Scribed by Prof. Dr. Wolfgang A. Herrmann; Roland A. Fischer; Dr. Eberhardf Herdtweck


Publisher
John Wiley and Sons
Year
1987
Tongue
English
Weight
361 KB
Volume
26
Category
Article
ISSN
0044-8249

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M, =72X.57: crystal dimensions: 0 2 x 0 2 x 0.2 mm; T = 200 K; (I = 20.951(6). h =10.973(9). c=16.770(8)&., {i=l0330(5)'. V = 3751.7(3)A3. 2 = 4. monoclinic. space group C2,c. P,,~, = 1.290 gem-? ~(Mo,,) = 1.875 inin ', CJ \can mode ( A w =1.1 ). 3,'$20145 . 5072 reflections were measured on a four-