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Alkylation of Aryl N-(2-Pyridylsulfonyl)aldimines with Organozinc Halides: Conciliation of Reactivity and Chemoselectivity

✍ Scribed by Jorge Esquivias; Ramón Gómez Arrayás; Juan Carlos Carretero

Publisher: John Wiley and Sons
Year: 2007
Tongue: English
Weight: 431 KB
Volume: 46
Category: Article
ISSN: 0044-8249
DOI: 10.1002/anie.200703239

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benzene gave orange crystals. M.p. 181 -185°C (decomp.); yield: 234.8 mg (70%). ## 4: A vigorously stirred solution of l(200 mg, 0.34 mmol) in toluene (10 ml) was treated with solid [Pt(PPh,),(C,H,),] (241.9 mg, 0.34 mmol) at 0°C. Upon addition, the solution immediately turned deep brown. After t