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Alcoholysis of Tetraphosphorus Heptasulfide P4S7

✍ Scribed by Dipl.-Chem. H. Petschik; Prof. Dr. E. Steger

Publisher
John Wiley and Sons
Year
1964
Tongue
English
Weight
139 KB
Volume
3
Category
Article
ISSN
0044-8249

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πŸ“œ SIMILAR VOLUMES

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ture-sensitive salt (Ic) is obtained after vacuum drying; m. p. 201-202 "C (decomposition above ca. 190 "C).

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By sulfur abstraction from a-P 4 S 9 /P 4 S 10 with triphenylphosphine a new phosphorus sulfide d-P 4 S 7 with adamantane skeleton and an additional sulfur in exo-position was identified in CS 2 -solution by 31 P-NMR spectroscopy. Product distribution and 31 P-NMR parameter are given.

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(CuI)(3)P(4)S(4) is obtained by reaction of stoichiometric amounts of CuI, P, and S in evacuated silica ampoules. The yellow compound consists of monomeric beta-P(4)S(4) cage molecules that are separated by hexagonal columns of CuI. (CuI)(3)P(4)S(4) crystallizes isotypic to (CuI)(3)P(4)Se(4) in the