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Additions and Corrections - Steroidal Heterocycles. 14. 1,8a-Epoxy-1,4-4a,5,6,7,8,8a-octahydro-2-hydroxynapthalene-3-carbonitrile and Related Compounds

✍ Scribed by Neumann, H.


Book ID
127302446
Publisher
American Chemical Society
Year
1972
Tongue
English
Weight
73 KB
Volume
15
Category
Article
ISSN
0022-2623

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The title compound, C 21 H 20 ClN 3 O 2 , was synthesized by the reaction of 4-chlorobenzaldehyde and 3-(5,5-dimethyl-3-oxocyclohex-1-enylamino)propanoic acid with malononitrile in ethylene glycol under microwave irradiation. The dihydropyridine ring has a boat conformation. The pyrimidine ring adop