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ChemInform Abstract: Synthesis of 5-Oxo-1,2,3,5,6,7-hexahydroimidazo(1,2-a)pyridine-8- carbonitriles, 6-Oxo-2,3,4,6,7,8-hexahydro-1H-pyrido(1,2-a)pyrimidine- 9-carbonitriles, and 7-Oxo-1,2,3,4,5,7,8,9-octahydropyrido(1,2-a)(1,3) diazepine-10-carbonitriles.

✍ Scribed by P. VICTORY; N. BUSQUETS; J. I. BORRELL; J. TEIXIDO; C. DE ALVARO; A. ARENAS; A. ALVAREZ-LARENA; J. F. PINIELLA


Book ID
112027945
Publisher
John Wiley and Sons
Year
2010
Weight
30 KB
Volume
27
Category
Article
ISSN
0931-7597

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✍ Chen, Dong-Qin ;Li, Chun-Mei ;Tu, Shu-Jiang πŸ“‚ Article πŸ“… 2007 πŸ› International Union of Crystallography 🌐 English βš– 873 KB

The title compound, C 21 H 20 ClN 3 O 2 , was synthesized by the reaction of 4-chlorobenzaldehyde and 3-(5,5-dimethyl-3-oxocyclohex-1-enylamino)propanoic acid with malononitrile in ethylene glycol under microwave irradiation. The dihydropyridine ring has a boat conformation. The pyrimidine ring adop