A total synthesis of [9′, 10′-3H]-labell
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Boguslaw Wichrowski; Elie Michel; Françoise Heymans; Jean Roy; Jean-Louis Morgat
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Article
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1983
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John Wiley and Sons
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French
⚖ 266 KB
l-O-octadecen-[9',1O']-yl 2-0-benzyl sn-glycero-3-phosrylcholine was obtained from I-O-octadecen-[9',10'I-yl sn-glycerol by tritylation, benzylation and phosphorylation with 2-bromoethyl phosphoryl dichloride followed with trimethylamine reaction. Catalytic tritiation o f the double bond led to lab