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Acetone (2-nitro­phen­yl)hydrazone

✍ Scribed by Jian, Fang-Fang ;Zhuang, Rui-Rui ;Wang, Ke-Fei ;Zhao, Pu-Su ;Xiao, Hai-Lian


Publisher
International Union of Crystallography
Year
2006
Tongue
English
Weight
63 KB
Volume
62
Category
Article
ISSN
1600-5368

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✦ Synopsis


The title compound, C 9 H 11 N 3 O 2 , was prepared by the reaction of 1-(2-nitrophenyl)hydrazine with acetone at room temperature. The molecule is approximately planar and exhibits a weak intramolecular hydrogen-bond interaction.


📜 SIMILAR VOLUMES


Acetone 2-nitro­phenyl­hydrazone
✍ Wardell, Solange M. S. V. ;Wardell, James L. ;Low, John N. ;Glidewell, Christoph 📂 Article 📅 2007 🏛 International Union of Crystallography 🌐 English ⚖ 161 KB
1-(4-Amino­phen­yl)-2-(4-nitro­phen­yl)e
✍ Li, Zong-Sheng ;Chai, Jian-She 📂 Article 📅 2007 🏛 International Union of Crystallography 🌐 English ⚖ 177 KB

In the title compound, C~14~H~12~N~2~O~3~, the dihedral angle between the two aromatic rings is 86.13 (15)°. Intermolecular N—H...O hydrogen bonds [N...O = 2.886 (3) Å and N—H...O = 174 (3)°] between the NH~2~ and C=O groups link the molecules into a one-dimensional ribbon augmented by secondary N—H

2-(3-Nitro­phen­yl)-2-oxazoline
✍ Decken, Andreas ;Botelho, Laura ;Sadowy, Amber L. ;Yadav, Paras N. ;Gossage, Rob 📂 Article 📅 2006 🏛 International Union of Crystallography 🌐 English ⚖ 102 KB

The title compound, C 9 H 8 N 2 O 3 , was obtained by a zinc chloride-promoted addition and ring-closure reaction involving 3-nitrobenzonitrile and 2-ethanolamine. The planar oxazoline and aromatic rings of the molecule are almost coplanar, with a dihedral angle of 8.79 (5) between them. The oxazoli

Benzyl­idene­acetone 2,4-di­nitro­phenyl
✍ Shan, Shang ;Fan, Zheng ;Hu, Wei-Xiao ;Xu, Duan-Jun 📂 Article 📅 2004 🏛 International Union of Crystallography 🌐 English ⚖ 216 KB

Single-crystal X-ray study T = 295 K Mean '(C±C) = 0.003 A Ê R factor = 0.048 wR factor = 0.127 Data-to-parameter ratio = 12.4 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.