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A water 17O NMR study of the pH dependent properties of superoxide dismutase

✍ Scribed by I. Bertini; C. Luchinat; L. Messori

Book ID
118315642
Publisher
Elsevier Science
Year
1981
Tongue
English
Weight
382 KB
Volume
101
Category
Article
ISSN
0006-291X

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## Abstract ^17^O‐enriched acetic acid (2.5% in ^17^O) was synthesized by hydrolysis of acetic anhydride with ^17^O‐enriched water. The reaction was monitored by ^17^O and ^1^H NMR spectroscopy. Acetic anhydride, ^17^O‐enriched in both the ether and the carbonyl oxygens, was observed as an intermed